Flash Vaporizer Injection Port

The flash vaporizer injection port instanteneously vaporizes the injected sample before it is introduced onto the column. This is achieved by maintaining a temperature of the port that is higher that the highest boiling substituent in the sample, often around 150oC.

Things to notice are:

  1. When injecting a liquid or vapor, a quick expansion of the volume occurs upon injection due to the evaporation of the liquid and at the same time increase in the temperature, which makes the vapor itself expand.
  2. When a liquid is inject a little bit will remain inside the needle of the syringe. This means that in order to have the narrowest plug introduced on the column one needs to avoid that material from more slowly evaporating and 'leaking' into the injection port, i.e., one should retract the needle immediately after the material is injected.
  3. Depending on the detector used, one can also make sure that a little bit of air is present in the syringe so that the retention time of an non-retained compound can be determined at the same time.

The injection is done quickly emptying a syringe stuck through a septum (see the quicktime movie below)


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