Chem 227: Spring 2009 | Dr. Rusay | ||||
http://chemconnections.org/organic/chem227/ | |||||
Secs. 2944 & 3004 | Class: | TTh 12:30-1:45 | MA 245 | ||
Sec. 2944 | Lab: | MW 11:00-1:50 |
PS 209 |
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Sec. 3004 | Lab: | TTh
2:O0-4:50 |
PS 209 |
Week | Mon. | Tues. | Weds. | Thurs. | Fri. |
#1 | 12-Jan | 13-Jan | 14-Jan | 15-Jan | 16-Jan |
Class |
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DUE before
next class: |
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Lab |
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#2 | 19-Jan | 20-Jan | 21-Jan | 22-Jan | 23-Jan |
Class |
Holiday |
IR
Spectroscopy Mass
Spectrometry (MS) NMR Introduction 1H NMR Spectrocopy.pdf |
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NMR
Introduction 1H NMR
Spectroscopy 1H NMR
Interpretation
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Lab | DUE -22 Jan Refer to: |
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Refer to: _____________ 1H NMR Lab 1H NMR
Tutorial-1 Chem
226 Reactions Review |
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#3 | 26-Jan | 27-Jan | 28-Jan | 29-Jan |
30-Jan |
Class |
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Spectroscopy:
IR-MS-UV-NMR 13C NMR
Spectroscopy |
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Lab |
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Refer to: ____________ 1H NMR Lab 1H NMR
Tutorial-1 Chem 226 Reactions Review IR/UV/MS
Worksheet Part I & Part II .pdf
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR
Spectroscopy 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf |
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#4 | 2-Feb | 3-Feb | 4-Feb | 5-Feb |
6-Feb |
Class |
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Chapter 11 Aromaticity Aromaticity
Worksheet Aromatic Reactions Naming Aromatics QUIZ: Aromaticity
Worksheet |
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Chapter
11 Aromaticity Aromatic
Reactions Electrophilic Aromatic Substitution I Naming Aromatics QUIZ: |
Holiday |
Lab |
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13C NMR
Spectroscopy 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf
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Run NMRs:1H & 13C of individual Unknowns 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy
and Reaction Chemistry: Analysis of a Draft for Publication -
pdf |
Run NMRs:1H & 13C of individual Unknowns 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf
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Results
(structures) of individual
Unknowns Peer Review: Analysis
of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf
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#5 | 9-Feb | 10-Feb | 11-Feb | 12-Feb | 13-Feb |
Class |
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Aromaticity
Worksheet Electrophilic Aromatic Substitution II
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Electrophilic Aromatic Substitution
II Electrophilic Aromatic Substitution III
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Last Day to Drop without a W |
Lab |
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Results
(structures) of individual Unknowns Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE DUE 2-Mar
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Results (structures) of individual Unknowns Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 26-Feb
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 2-Mar
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 26-Feb |
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#6 | 16-Feb | 17-Feb | 18-Feb | 19-Feb | 20-Feb |
Class |
Holiday |
Electrophilic Aromatic Substitution
(EAS) III EAS: Practice Questions
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EXAM
1: EAS: Practice Questions Electrophilic
Aromatic Substitution Worksheet .pdf
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Lab |
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 26-Feb |
Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 2-Mar
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 26-Feb |
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#7 | 23-Feb | 24-Feb | 25-Feb | 26-Feb | 27-Feb |
Class |
Carbonyls: Aldehydes & Ketones (Chap.17)
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Carbonyls: Aldehydes & Ketones (Chap.17) Aldehydes & Ketones
I Aldehydes & Ketones
II Worksheet: Due
5-Mar |
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Lab | |||||
Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 26-Feb
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 2-Mar
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Chiral Compounds and Green Chemistry Introduction/Handout ___________ Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE TODAY |
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#8 | 2-Mar | 3-Mar | 4-Mar | 5-Mar | 6-Mar |
Class |
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Carbonyls: Aldehydes & Ketones (Chap.17) Aldehydes & Ketones
I Aldehydes & Ketones
II Worksheet: Due
5-Mar
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Carbonyls: Aldehydes & Ketones
Enols & Enolates(Chaps.18 & 21) Worksheet: Due |
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Lab | |||||
Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE TODAY Chiral Compounds and Green Chemistry Introduction/Handout |
Electrophilic Aromatic Substitution / Friedel Crafts Acylation: Synthesis Project Debriefing Chiral Compounds and Green Chemistry: Pre-lab due; set up/ Characterization Aldol
Condensation DUE 12
Mar
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Electrophilic Aromatic Substitution / Friedel Crafts Acylation: Synthesis Project Debriefing Chiral Compounds and Green Chemistry: Pre-lab due; set up/ Characterization Aldol
Condensation DUE 16
Mar |
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Enolates
(Molecular Modeling) |
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#9 | 9-Mar | 10-Mar | 11-Mar | 12-Mar | 13-Mar |
Class |
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Enols & Enolates(Chaps.18 & 21) Worksheet: Due
Today |
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Enols & Enolates(Chaps.18 &21) Synthesis and Reactions of beta-Dicarbonyl Compounds WKS .pdf Due 19-Mar |
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Lab | |||||
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Enolates
(Molecular Modeling) |
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Aldol
Condensation DUE 12
Mar |
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Aldol
Condensation DUE 16
Mar |
Chiral
Compounds and
Green Chemistry: Report Due Aldol
Condensation DUE LIBRARY
Research Project
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#10 | 16-Mar | 17-Mar | 18-Mar | 19-Mar | 20-Mar |
Class |
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Enols & Enolates(Chaps.18 &21) Carboxylic
Acids & Derivatives (Chaps.19&20) Acids-Derivatives
Spectroscopy LIBRARY
Research Project Start: CPR:
Design and Development of Drugs
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Carboxylic Acids & Derivatives
(Chaps.19&20) Acids-Derivatives
Spectroscopy Carboxylic Acids Worksheet .pdf Due 31-Mar Synthesis and Reactions of beta-Dicarbonyl Compounds WKS .pdf Due Today LIBRARY
Research Project CPR:
Design and Development of Drugs
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LIBRARY
Research Project CPR: Design and Development of Drugs Complete Text Entry before 11:55 PM: Monday, 23-Mar Complete Assignment (DUE 11:55 PM Apr 1) |
Lab | |||||
Chiral
Compounds and
Green Chemistry: Report DUE Aldol
Condensation DUE LIBRARY
Research Project
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Chiral
Compounds and
Green Chemistry: Report Due Friday 20-Mar 3:00PM Aldol
Condensation DUE LIBRARY
Research Project
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Chiral
Compounds and
Green Chemistry: Report Due Friday 20-Mar 3:00PM Aldol
Condensation DUE LIBRARY
Research Project
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Dimedone
Synthesis |
Chiral
Compounds and
Green Chemistry: Report Due Today 3:00PM
Aldol
Condensation DUE Today 3:00PM LIBRARY
Research Project |
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#11 | 23-Mar | 24-Mar | 25-Mar | 26-Mar | 27-Mar |
Class | LIBRARY
Research Project DVC/ UC Berkeley CPR:
Design and Development of Drugs
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LIBRARY Research
Project DVC/ UC Berkeley CPR: Design and Development of Drugs Complete Assignment (before 11:55 PM, 1-Apr) |
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Dr. Kutner (PS-217)
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CPR:
Design and Development of Drugs |
Lab | |||||
LIBRARY Research
Project DVC/ UC Berkeley CPR:
Design and Development of Drugs |
LIBRARY
Research Project DVC/ UC Berkeley
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LIBRARY Research Project DVC/ UC Berkeley DVC LAB OPEN |
LIBRARY Research Project DVC/ UC Berkeley DVC
LAB OPEN (Dr. Kutner) |
CPR:
Design and Development of Drugs Complete Assignment (before 11:55 PM, 1-Apr) |
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#12 | 30-Mar | 31-Mar | 1-Apr | 2-Apr | 3-Apr |
Class |
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EXAM 2 Suggested review: Carboxylic Acids Worksheet .pdf Due Today Library
Research Project Assignment
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CPR: Design and Development of Drugs Complete Assignment (before 11:55 PM, TODAY)
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Carboxylic
Acids & Derivatives
(Chaps.19&20) Carboxylic Acids & Derivatives Carboxylic Acid Derivatives Worksheet .pdf Due 9-Apr Carboxylic Acid Derivatives:
Addition-Elimination & Synthesis (Individual)
Worksheet
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Lab | |||||
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#13 | 6-Apr | 7-Apr | 8-Apr | 9-Apr | 10-Apr |
Class |
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Carboxylic Acids & Derivatives
(Chap. 20) Chapter 23: Nucleophilic Aromatic Substitution Nucleophilic Aromatic Substitution Worksheet .pdf DUE 21-April Substitution / Bottlebrush
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Carboxylic
Acids & Derivatives (Chap. 20) Chapter
23: Nucleophilic Aromatic Substitution Chapter
24: Phenols Library
Research Project Carboxylic Acid Derivatives Worksheet .pdf Due Today Carboxylic Acid Derivatives:
Addition-Elimination & Synthesis (Individual)
Worksheet
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Lab | |||||
Dimedone Post lab DEET
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Dimedone Post lab DEET
|
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#14 | 13-Apr | 14-Apr | 15-Apr | 16-Apr | 17-Apr |
Class | Holiday | Holiday
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Holiday |
Holiday
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Holiday |
Lab | |||||
#15 | 20-Apr | 21-Apr | 22-Apr | 23-Apr | 24-Apr |
Class |
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Chapter
24: Phenols (Quinones) Chapter 22: Amines Amine Worksheet Nucleophilic Aromatic Substitution Worksheet .pdf DUE Today |
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Chapter
22: Amines Chapter 25: Carbohydates Carbohydrates III Class Carbohydrates WKS DUE 30-Apr |
Last Day to Drop with a W |
Lab | |||||
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DEET Report
& Samples
Separation & Identification of Unknowns
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DEET Report & Samples
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#16 | 27-Apr | 28-Apr | 29-Apr | 30-Apr | 1-May |
Class |
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Chapter
25: Carbohydates Carbohydrates WKS DUE 30-Apr Chapter
26: Lipids Review: Lipids Wordsearch DUE 5-May Amine Worksheet
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Chapter
26: Lipids Review: Lipids Wordsearch DUE 5-May Chapter
27: Amino Acids / Proteins Amino Acid Table .pdf DUE
4 or 5-May
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Lab | |||||
Chapter
29: Synthetic Polymers POLYMER CHEMISTRY: Nylon/Slime/ Silly
Putty
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i-clicker class questions quiz: Chapter 22, Amines & Chapter 25, Carbohydrates Chapter 29: Polymers POLYMER CHEMISTRY: Nylon/Slime/ Silly Putty Separation & Identification of Unknowns: High resolution MS Molecular ion data
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i-clicker class questions quiz: Chapter 22, Amines & Chapter 25, Carbohydrates POLYMER CHEMISTRY: Nylon/Slime/ Silly Putty Due TODAY Chapter 27: Amino Acids
/ Proteins Discussion: Separation & Identification of Unknowns: High resolution MS Molecular ion data
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POLYMER CHEMISTRY: Nylon/Slime/ Silly Putty Due TODAY Chapter 27: Amino Acids
/ Proteins Discussion: Separation & Identification of Unknowns: High resolution MS Molecular ion data
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#17 | 4-May | 5-May | 6-May | 7-May | 8-May |
Class |
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Chapter
27: Amino Acids / Proteins Amino Acids & Protein i-clicker Questions _________ Protein-synthesis.pdf Lipids
Wordsearch DUE
Today |
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Lab | |||||
Separation & Identification of Unknowns: High resolution MS Molecular ion data
Chapter 27: Amino Acids
/ Proteins 1) Amino Acid Table Discussion: |
Separation & Identification of Unknowns: High resolution MS Molecular ion data
Chapter 27: Amino Acids
/ Proteins 1) Amino Acid Table
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Separation & Identification of Unknowns: High resolution MS Molecular ion data
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Separation & Identification of Unknowns: High resolution MS Molecular ion data
|
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#18 | 11-May | 12-May | 13-May | 14-May | 15-May |
Class |
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EXAM
3 Additional Suggested Problems:
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Must be present for credit.
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DUE 12:00
noon Separation & Identification of Unknowns |
Lab | Separation & Identification of Unknowns: High resolution MS Molecular ion data
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Separation & Identification of Unknowns: High resolution MS Molecular ion data
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Lab Check In |
End
of Course Survey Lab Check In DVC Science Alumni: |
Separation & Identification
of Unknowns:
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#19 | 18-May | 19-May | 20-May | 21-May | 22-May |
Class |
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FINAL
EXAM DUE: |
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