Chem 227: Spring 2010 | Dr. Rusay | ||||
http://chemconnections.org/organic/chem227/ | |||||
Secs. 2944 & 3004 | Class: | TTh 12:30-1:45 | PS 277 | ||
Sec. 2944 | Lab: | MW 11:00-1:50 |
PS 209 |
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Sec. 3004 | Lab: | TTh
2:O0-4:50 |
PS 209 |
Week | Mon. | Tues. | Weds. | Thurs. | Fri. |
#1 | 25-Jan | 26-Jan | 27-Jan | 28-Jan | 29-Jan |
Class |
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DUE before
next class: |
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Must
have and use i-clicker to
receive class credit. IR
Spectroscopy IR-Cards NMR
Introduction 1H NMR Spectrocopy.pdf |
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Lab |
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Check out
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#2 | 1-Feb | 2-Feb | 3-Feb | 4-Feb | 5-Feb |
Class |
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NMR
Introduction 1H NMR
Spectroscopy 1H NMR
Interpretation Worksheet:
Chem 121 Review Problems |
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1H NMR
Spectroscopy 1H NMR
Interpretation Worksheet:
Chem 121 Review Problems
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Lab |
Refer to: |
High Res. MS Data Refer to: |
Mass
Spectrometry (MS) 1H NMR Lab
Begin running NMRs:1H & 13C of
individual Unknowns |
Mass
Spectrometry (MS) 1H NMR Lab 1H NMR
Spectroscopy Chem
226 Reactions Review Begin
running NMRs:1H & 13C of
individual Unknowns |
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#3 | 8-Feb | 9-Feb | 10-Feb | 11-Feb |
12-Feb |
Class |
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Spectroscopy:
IR-MS-UV-NMR 13C NMR
Spectroscopy
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Spectroscopy
QUIZ: Chapter
11 Aromaticity Aromaticity
Worksheet Aromatic
Reactions Naming Aromatics
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Holiday |
Lab |
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR
Spectroscopy 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Running
NMRs:1H & 13C of
individual Unknowns |
1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR
Spectroscopy 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Running
NMRs:1H & 13C of
individual Unknowns
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Running
NMRs:1H & 13C of
individual Unknowns
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1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Running
NMRs:1H & 13C of
individual Unknowns |
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#4 | 15-Feb | 16-Feb | 17-Feb | 18-Feb |
19-Feb |
Class |
Holiday
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Chapter 11 Aromaticity Aromatic
Reactions Aromaticity update Electrophilic Aromatic Substitution
I Naming Aromatics QUIZ:
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Aromaticity
Worksheet Electrophilic Aromatic Substitution
II
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Last Day to Drop without a W |
Lab |
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Running
NMRs:1H & 13C of
individual Unknowns 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy
and Reaction Chemistry: Analysis of a Draft for Publication -
pdf |
Running
NMRs:1H & 13C of
individual Unknowns 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf
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Peer Review: Analysis
of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf INTRODUCTION: Samples DUE 11-Mar
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#5 | 22-Feb | 23-Feb | 24-Feb | 25-Feb | 26-Feb |
Class |
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Electrophilic Aromatic Substitution
(EAS) III EAS: Practice Questions |
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Lab |
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Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 15-Mar |
Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 11-Mar
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Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 15-Mar
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar |
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#6 | 1-Mar | 2-Mar | 3-Mar | 4-Mar | 5-Mar |
Class |
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EXAM
1: Sample Test w/o answers EAS: Practice Questions Electrophilic
Aromatic Substitution Worksheet .pdf
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Carbonyls: Aldehydes & Ketones (Chap.17)
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Lab |
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Project Instructions .pdf Samples DUE 15-Mar
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CANCELLED Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE |
Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 15-Mar
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE |
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#7 | 8-Mar | 9-Mar | 10-Mar | 11-Mar | 12-Mar |
Class | Carbonyls: Aldehydes & Ketones (Chap.17) Aldehydes & Ketones
I Aldehydes & Ketones
II Worksheet: Due
18-Mar
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Carbonyls: Aldehydes & Ketones
(Chap.17) Aldehydes & Ketones
I Aldehydes & Ketones
II Worksheet: Due
18-Mar Enols & Enolates(Chaps.18 & 21)
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Lab | |||||
Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar
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Chiral Compounds and Green Chemistry Introduction/Handout ___________ Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE Today
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Chiral Compounds and Green Chemistry Introduction/Handout ___________ Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE TODAY |
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#8 | 15-Mar | 16-Mar | 17-Mar | 18-Mar | 19-Mar |
Class |
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Carbonyls: Aldehydes & Ketones Worksheet: Due
Mar 18 Enols & Enolates(Chaps.18 & 21) Worksheet: Due
25-Mar
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Enols & Enolates(Chaps.18 & 21) Worksheet: Due
Today
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Lab | |||||
Chiral Compounds and Green Chemistry: Pre-lab due; set up/ Characterization Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Report DUE TODAY
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Chiral Compounds and Green Chemistry: Pre-lab due; set up/ Characterization Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Report DUE TODAY
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Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Enolates
(Molecular Modeling) |
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Enolates
(Molecular Modeling) |
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#9 | 22-Mar | 23-Mar | 24-Mar | 25-Mar | 26-Mar |
Class |
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Enols & Enolates(Chaps.18 &21) Worksheet: Due
25-Mar Synthesis and Reactions of beta-Dicarbonyl Compounds WKS .pdf Due 1-Apr |
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Enols & Enolates(Chaps.18 &21) Synthesis
and Reactions of beta-Dicarbonyl Compounds WKS Due
1-Apr Carboxylic Acids & Derivatives (Chaps.19&20) Acids-Derivatives
Spectroscopy
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Lab | |||||
Electrophilic Aromatic Substitution / Friedel Crafts Acylation: Synthesis Project Debriefing Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Enolates
(Molecular Modeling) |
Electrophilic Aromatic Substitution / Friedel Crafts Acylation: Synthesis Project Debriefing Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Aldol
Condensation |
Chiral
Compounds and
Green Chemistry: Continuation/ Characterization Aldol
Condensation DUE 1-Apr |
Chiral Compounds and Green Chemistry: Report DUE 1-Apr Aldol
Condensation DUE 1-Apr
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#10 | 29-Mar | 30-Mar | 31-Mar | 1-Apr | 2-Apr |
Class |
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Carboxylic Acids & Derivatives (Chaps.19&20) Carboxylic
Acids & Derivatives Carboxylic Acid Derivatives Worksheet .pdf Due 15-Apr Carboxylic Acid Derivatives:
Addition-Elimination & Synthesis (Individual)
Worksheet
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Carboxylic
Acids & Derivatives (Chaps.19&20) Carboxylic
Acids & Derivatives Carboxylic Acid Derivatives Worksheet .pdf Due 15-Apr Carboxylic Acid Derivatives:
Addition-Elimination & Synthesis (Individual)
Worksheet ___________ Staph resistance- vancomycin- synthesis Chapter 23: Nucleophilic Aromatic Substitution Substitution
/ Bottlebrush Chiral Compounds and Green Chemistry: Report Due Today Aldol
Condensation DUE Today Synthesis
and Reactions of beta-Dicarbonyl Compounds WKS .pdf Due
Today |
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Lab | |||||
Ester
Hydrolysis Chiral Compounds and Green Chemistry: Report Due 1-Apr 5:00PM Aldol
Condensation Due 1-Apr 5:00PM
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Ester
Hydrolysis Chiral Compounds and Green Chemistry: Report Due 1-Apr 5:00PM Aldol
Condensation Due 1-Apr 5:00PM |
Ester
Hydrolysis Due 12-Apr Chiral Compounds and Green Chemistry: Report Due 1-Apr 5:00PM Aldol
Condensation Due 1-Apr 5:00PM |
Ester
Hydrolysis Due 13-Apr Chiral Compounds and Green Chemistry: Report Due TODAY 5:00PM Aldol
Condensation Due TODAY 5:00PM |
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#11 | 5-Apr | 6-Apr | 7-Apr | 8-Apr | 9-Apr |
Class | Spring Break
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#12 | 12-Apr | 13-Apr | 14-Apr | 15-Apr | 16-Apr |
Class |
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Carboxylic Acids & Derivatives (Chaps.19&20) Carboxylic
Acids & Derivatives Carboxylic Acid Derivatives Worksheet .pdf Due 15-Apr Carboxylic Acid Derivatives:
Addition-Elimination & Synthesis (Individual)
Worksheet Staph resistance- vancomycin- synthesis Chapter 23: Nucleophilic Aromatic Substitution Nucleophilic Aromatic Substitution Worksheet .pdf DUE 22-April Substitution
/ Bottlebrush
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EXAM
2 Practice Questions .pdf RESULTS Carboxylic Acids Worksheet .pdf Due Today Exploration
3-form .pdf Carboxylic Acid Derivatives Worksheet .pdf Due TODAY |
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Lab | |||||
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Literature
research Compound Selection: Due TODAY Report Due 5:00 PM 30-Apr |
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#13 | 19-Apr | 20-Apr | 21-Apr | 22-Apr | 23-Apr |
Class |
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Chapter 23: Nucleophilic Aromatic Substitution Nucleophilic Aromatic Substitution Worksheet .pdf DUE 22-April Substitution
/ Bottlebrush Chapter 24: Phenols Phenols & Amines
Worksheet |
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Chapter 24: Phenols Chapter 22: Amines Phenols & Amines
Worksheet Nucleophilic Aromatic Substitution Worksheet .pdf DUE Today
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Lab | |||||
Dimedone SLO DEET Completion: Carboxylic Acid Derivatives Worksheet .pdf (Due 15-Apr!!) |
Dimedone SLO DEET Completion: Carboxylic Acid Derivatives Worksheet .pdf (Due 15-Apr!!) |
Separation & Identification of
Unknowns
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Separation & Identification of
Unknowns High resolution MS Molecular ion data
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#14 | 26-Apr | 27-Apr | 28-Apr | 29-Apr | 30-Apr |
Class |
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Chapter 22: Amines
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Chapter 25: Carbohydates
Phenols & Amines
Worksheet
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Lab | |||||
Separation & Purification of
Unknowns
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Separation & Purification of
Unknowns
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Separation & Purification of
Unknowns High resolution MS Molecular ion data
| Separation & Purification of
Unknowns
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#15 | 3-May | 4-May | 5-May | 6-May | 7-May |
Class |
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Chapter 25: Carbohydates
Chapter 26: Lipids Review: |
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Chapter 25: Carbohydates
Chapter
26: Lipids Review: Lipids Wordsearch DUE May 13 Carbohydrates
WKS DUE
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Lab | |||||
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(Carey;
Chapter 29)
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(Carey;
Chapter 29) Polymers ppt Polymers pdf Polymers Lab
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#16 | 10-May | 11-May | 12-May | 13-May | 14-May |
Class |
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Carbohydrates WKS DUE Today Chapter 26: Lipids Review: Chapter 27: Amino Acids / Proteins Amino
Acids & Protein i-clicker Questions _________ |
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Chapter
28: Nucleosides, DNA & RNA DNA i-clicker
Questions Lipids
Wordsearch DUE
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Exam
3 Help Session See: Amino
Acids & Protein i-clicker Questions |
Lab | |||||
Chapter
27: Amino Acids / Proteins
(Carey;
Chapter 29) |
Chapter
27: Amino Acids / Proteins
(Carey;
Chapter 29) |
Chapter
27: Amino Acids / Proteins 1) Amino Acid Table (Carey;
Chapter 29) |
Chapter
27: Amino Acids / Proteins 1)
Amino Acid Table (Carey;
Chapter 29) |
Exam
3 Help Session See: Amino
Acids & Protein i-clicker Questions DNA i-clicker Questions
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#17 | 17-May | 18-May | 19-May | 20-May | 21-May |
Class |
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EXAM
3 Additional Suggested Problems: Lipids Wordsearch DUE Today |
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Must be present for credit.
Dress-up Thursday & Some Lab Photos courtesy of Indah
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Separation & Purification of
Unknowns Report
form |
Lab | |||||
Protein Chemistry: Amino Acids, Flour, Dough & Elasticity Protein-synthesis.pdf Separation & Purification of
Unknowns
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Protein Chemistry: Amino Acids, Flour, Dough & Elasticity Separation & Purification of
Unknowns
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Lab Check In |
Lab Check In Separation & Purification of
Unknowns Report
form |
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#18 | 24-May | 25-May | 26-May | 27-May | 28-May |
Class |
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FINAL EXAM |
ACS Exam |
Lab | |||||
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