Chem 227: Spring 2013 | Dr. Rusay | ||||
http://chemconnections.org/organic/chem227/ | |||||
Secs. 2944 & 3004 | Class: | TTh 9:30-11:45 | PS 275 | ||
Sec. 2944 | Lab: | MW
11:00-1:50 |
PS 209 |
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Sec. 3004 | Lab: | MW
2:30-5:20 |
PS 209 |
Week | Mon. | Tues. | Weds. | Thurs. | Fri. |
#1 | 14-Jan | 15-Jan | 16-Jan | 17-Jan | 18-Jan |
Class |
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Organic Chemistry II: Expanding & Connecting IR
Spectroscopy IR Handout IR-Cards DUE before 17-Jan class:
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DUE TODAY before class: Must have and use i-clicker to receive class participation credit. IR
Spectroscopy IR Handout IR-Cards Mass
Spectrometry (MS) |
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Lab |
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IR
Spectroscopy IR Handout IR-Cards Mass
Spectrometry (MS) DUE before 17-Jan class:
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#2 | 21-Jan | 22-Jan | 23-Jan | 24-Jan | 25-Jan |
Class |
Holiday |
IR i-clicker Quiz Mass
Spectrometry (MS) 1H NMR
Spectroscopy 1H NMR
Interpretation Worksheet:
Chem 121 Review Problems |
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Mass
Spectrometry (MS) Worksheet:
Chem 121 Review Problems
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Lab |
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Refer to:
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#3 | 28-Jan | 29-Jan | 30-Jan | 31-Jan |
1-Feb |
Class |
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Spectroscopy:
IR-MS-UV-NMR 13C NMR
Spectroscopy
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13C NMR
Spectroscopy Spectroscopy
on-line QUIZ 1.2: Naming Aromatics
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Last Day to Drop without a W |
Lab |
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Worksheet Part
I & Part II .pdf 1H NMR
Spectroscopy 1H NMR
Interpretation 1H NMR Lab
Begin running NMRs:1H & 13C of
individual Unknowns 13C NMR
Spectroscopy 13C NMR Lab
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Spectroscopy in-class QUIZ 1.1 Spectroscopy
on-line QUIZ 1.2: 1H NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf 13C NMR
Spectroscopy 13C NMR Lab 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Running
NMRs:1H & 13C of
individual Unknowns
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#4 | 4-Feb | 5-Feb | 6-Feb | 7-Feb |
8-Feb |
Class | Chapter 18: Aromaticity
Worksheet Aromatic
Reactions Naming Aromatics
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Aromaticity
Worksheet Electrophilic Aromatic Substitution
II
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Lab |
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13C NMR
Spectroscopy 13C NMR Data 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Spectroscopy
on-line QUIZ 1.2: Running
NMRs:1H & 13C of
individual Unknowns Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf |
Spectroscopy
on-line QUIZ 1.2: Running
NMRs:1H & 13C of
individual Unknowns 13C NMR
Spectrosopy: Interpretation / Prediction & Reactions Lab Worksheet .pdf Peer Review: Analysis of a Draft for Publication Integrated Spectroscopy and
Reaction Chemistry: Analysis of a Draft for Publication - pdf
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#5 | 11-Feb | 12-Feb | 13-Feb | 14-Feb | 15-Feb |
Class |
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Electrophilic Aromatic Substitution
III EAS: Practice Questions Nucleophilic Aromatic Substitution |
Holiday
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Lab |
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Aromatic
Reactions Electrophilic Aromatic Substitution
I Aromaticity
Worksheet Practice Problems (fid files) Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 11-Mar |
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Electrophilic
Aromatic Substitution Worksheet .pdf Peer Review: Analysis of
a Draft for Publication Integrated
Spectroscopy and Reaction Chemistry: Analysis of a Draft for Publication -
pdf INTRODUCTION: Samples DUE 11-Mar
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#6 | 18-Feb | 19-Feb | 20-Feb | 21-Feb | 22-Feb |
Class |
Holiday |
EXAM
1: Sample Test w/o answers EAS: Practice Questions Comprehensive + selected [Chapters: 15, 16, 18, 19] Electrophilic
Aromatic Substitution Worksheet .pdf
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Nucleophilic Aromatic Substitution Chapter 17:
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Lab |
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Electrophilic
Aromatic Substitution Worksheet .pdf Begin Synthesis Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar
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#7 | 25-Feb | 26-Feb | 27-Feb | 28-Feb | 1-Mar |
Class | Chapter 17: Nucleophilic Aromatic Substitution WKS .pdf
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Carbonyls: Aldehydes & Ketones
(Chapter 20) Questions & Guide: Aldehydes & Ketones
I Aldehydes & Ketones
II Worksheet: Due
11-Mar
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Lab | |||||
Nucleophilic Aromatic Substitution Nucleophilic Aromatic Substitution WKS .pdf Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar
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Electrophilic
Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar Nucleophilic Aromatic Substitution WKS .pdf
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#8 | 4-Mar | 5-Mar | 6-Mar | 7-Mar | 8-Mar |
Class |
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Carbonyls: Aldehydes & Ketones Worksheet: Due
11-Mar Enols & Enolates(Chap. 22) Worksheet:Due 3-Apr
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Aldehydes & Ketones
II Questions & Guide: Worksheet: Due
11-Mar Enols & Enolates(Chap. 22) Questions & Guide: Worksheet: Due
11-Mar |
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Lab | |||||
Diels
Alder / Periccylclic Reactions Nucleophilic Aromatic Substitution WKS .pdf Electrophilic Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar
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Diels Alder / Periccylclic Reactions Diels
Alder / Molecular Modeling / Synthesis Electrophilic Aromatic Substitution / Friedel Crafts Acylation Synthesis Project Samples DUE 11-Mar
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#9 | 11-Mar | 12-Mar | 13-Mar | 14-Mar | 15-Mar |
Class |
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Enols & Enolates (Chap. 22) Questions & Guide: Worksheet: Due 3-Apr Synthesis and Reactions of beta-Dicarbonyl Compounds WKS Due 3-Apr |
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Enols & Enolates(Chap. 22) Questions & Guide: Synthesis and Reactions of beta-Dicarbonyl Compounds WKS Due 3-Apr
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Lab | |||||
Electrophilic Aromatic Substitution / Friedel Crafts Acylation: Synthesis Project Debriefing Samples DUE TODAY Diels Alder / Periccylclic Reactions Enolates
Aldehyde & Ketone
Syntheses WKS.pdf DUE
27-Mar
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Enolates
Aldehyde & Ketone
Syntheses WKS.pdf DUE 27-Mar |
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#10 | 18-Mar | 19-Mar | 20-Mar | 21-Mar | 22-Mar |
Class | Spring Break
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#11 | 25-Mar | 26-Mar | 27-Mar | 28-Mar | 29-Mar |
Class |
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Carboxylic Acids & Derivatives
(Chapter 21) REVIEW: |
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Carboxylic Acids & Derivatives
(Chapter 21) Carboxylic
Acids & Derivatives |
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Lab | |||||
Part
4: Michael Addition & organocopper reactions Enolates Aldehyde & Ketone
Syntheses WKS.pdf DUE 27-Mar |
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Synthesis
of a bio-regulator Aldehyde & Ketone
Syntheses WKS.pdf DUE Today |
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#12 | 1-Apr | 2-Apr | 3-Apr | 4-Apr | 5-Apr |
Class |
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EXAM
2 [Chapters
17, 19:(Nucleophilic aromatic
substitution), 20, 21 (Carboxylic Acids only), 22.] Practice Questions .pdf |
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Questions & Guide: Carboxylic
Acids & Derivatives Staph resistance- vancomycin- synthesis
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Lab | |||||
Synthesis
of a bio-regulator Ester Hydrolysis Enolates
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Synthesis
of a bio-regulator Ester Hydrolysis Exploration
3 Enolates Worksheet: Due Today Synthesis
and Reactions of beta-Dicarbonyl Compounds WKS Due Today |
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#13 | 8-Apr | 9-Apr | 10-Apr | 11-Apr | 12-Apr |
Class | Questions & Guide: Carboxylic
Acids & Derivatives Staph resistance- vancomycin- synthesis Chapter 23: Amines
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Chapter
23: Amines Amines Worksheet .pdf Carboxylic
Acids pdf
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Lab | |||||
DEET Synthesis Prelab Synthesis
of a bio-regulator Ester
Hydrolysis Carboxylic Acid Derivatives Worksheet pdf DUE 11-Apr
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DEET Synthesis
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#14 | 15-Apr | 16-Apr | 17-Apr | 18-Apr | 19-Apr |
Class |
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Chapter
23: Amines Amines Worksheet .pdf
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Chapter
23: Amines Chapter
24: Carbohydrates Carbohydrates II ppt Carbohydrates Worksheet .pdf
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Lab | |||||
DEET Synthesis CPR: Design and Development of Drugs Literature
Research |
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QUIZ: Carboxylic
Acids Derivatives DEET Synthesis Report & Sample CPR:
Design and Development of Drugs Literature Research
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#15 | 22-Apr | 23-Apr | 24-Apr | 25-Apr | 26-Apr |
Class |
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Amines
Worksheet .pdf Chapter
24: Carbohydrates Carbohydrates III ppt Carbohydrates Worksheet .pdf |
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Chapter
24: Carbohydrates Chapter
26: Lipids
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Last day to drop w/o a W on transcript |
Lab | |||||
DEET Synthesis
Report & Sample Amines
Worksheet .pdf CPR:
Design and Development of Drugs Literature Research Chapter 24: Carbohydrates Flatulence: |
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Flatulence: CPR:
Design and Development of Drugs Literature Research |
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#16 | 29-Apr | 30-Apr | 1-May | 2-May | 3-May |
Class |
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Chapter
26: Lipids Lipids WKS |
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Chapter
26: Lipids Lipids WKS
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Lab | |||||
Strawberry DNA Extraction Carbohydrates Worksheet .pdf CPR:
Design and Development of Drugs Literature Research Unknown Mixtures Instructions pdf MS Data |
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Quiz: Saccharides & DNA/ i-clicker questions + Powerpoint Strawberry DNA Extraction Literature Research Flatulence Experiment: Unknown Mixtures Instructions pdf MS Data |
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#17 | 6-May | 7-May | 8-May | 9-May | 10-May |
Class |
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Chapter
25: Amino Acids / Proteins Part II ppt
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Chapter
25: Amino Acids / Proteins Chapter 26: Polymers(For final exam) i-Clicker Quiz (as time allows; otherwise on May 13): Lipids WKS
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OPEN Lab 9:00 AM - 3:00 PM |
Lab | |||||
Influenza Instructions pdf Unknown Mixtures Instructions pdf MS Data NMR labeled samples in color coded capped nmr tubes DUE 13-May: 1) neutral + TMS 2) 5% carboxylic acid solution + TMS Unknown Mixtures Results Form & Supporting Spectra with interpretations DUE 21-May Literature Research |
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IInfluenza Instructions pdf Unknown Mixture Samples and supporting Lab Notebook Pages DUE 15-May NMR labeled samples in color coded capped nmr tubes DUE 13-May: 1) neutral + TMS 2) 5% carboxylic acid solution + TMS Unknown Mixtures Results Form & Supporting Spectra with interpretations DUE 21-May Strawberry DNA Extraction Literature Research |
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#18 | 13-May | 14-May | 15-May | 16-May | 17-May |
Class |
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EXAM
3 Suggested Preparation: i-Clicker questions, Worksheets, Textbook homework problems Additional Suggested Problems: |
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Influenza Performances EXAM
3 Course Survey
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Lab | |||||
Influenza Instructions pdf Chapter 26: Polymers(For final exam) Unknown Mixture Samples and supporting Lab Notebook Pages DUE 15-May NMR labeled samples in color coded capped nmr tubes DUE Today: 1) neutral + TMS 2) 5% carboxylic acid solution + TMS Unknown Mixtures Results Form & Supporting Spectra with interpretations DUE 21-May Polymer Worksheet pdf |
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Lab Check In Unknown Mixture Samples and supporting Lab Notebook Pages DUE Today Unknown Mixtures Results Form & Supporting Spectra with interpretations DUE 21-May Polymer Worksheet pdfDUE 23-May |
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#19 | 20-May | 21-May | 22-May | 23-May | 24-May |
Course Survey If participating, * Fill in your email address * Enter the instrument number: 61157 * Provide the instrument password: chem227 DUE: 22-May |
Unknown Mixtures Results Form & Supporting Spectra with interpretations DUE Today Course Survey |
Course Survey If participating, * Fill in your email address * Enter the instrument number: 61157 * Provide the instrument password: chem227 DUE: TODAY |
Final Exam Polymer Worksheet pdf |
ACS Exam |
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